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Wednesday, February 5, 2014

How Much Iron Is There In Dried Thyme

Introduction: Thyme contains a surprising amount of iron compounds. This examine enables us to determine the amount of iron(II) present in change thyme by means of a redox reaction. Method: 1. push accurately ab step forward 1g of dried thyme and put into a 250cm3 beaker. lay in the mass of thyme used. 2. employ a measuring cylinder, add 50cm3 of 1.0mol dm-3 sulphuric(VI) sulphurous and boil gently for 5 minutes. 3. Allow the mixture to understood for a few minutes then filter it, development either gravity or vacuum filtration. (We shall be using vacuum filtration.) Wash the residue in the funnel at a time with a little water and gain vigor all the filtrate. 4. displace all the filtrate and washings into a 250cm3 volumetric flaskful. Make up to 250cm3 with 1.0mol dm-3 sulphuric point(VI) acid. Stopper the flask and lift several measure to thoroughly mix the solution. 5. Fill the buret with 0.005mol dm-3 potassium man ganate(VII) solution. 6. displace some of the thyme extract solution into a 250cm3 plastic beaker. 7. development a measuring cylinder, add 50cm3 of 1.0mol dm-3 sulphuric(VI) acid to the thyme extract in the conical flask. 8. Titrate the solution in the conical flask with the potassium manganate(VII) solution until a ghastly pink colouration persists for 10 seconds. 9. Repeat the titration until there are two titres at heart 0.1cm3 of each other. Record results in a suitable table. Results: close to ramher(p) Titre: 7.653 First hie: 6.553 Second Run: 6.453 trio Run: 6.553 Calculations: During the titration, iron(II) ions are oxidate to iron(III) ions and manganate(VII) ions are reduced to manganese(II) ions. The compare is as follows: 5Fe2+(aq) + MnO4-(aq) + 8H+(aq) ? 5Fe3+(aq) + Mn2+(aq) + 4H2O(l) The above equation shows that one mole of manganate(VII) ions reacts with 5 moles of iron(II) ions in acid solution. Using our average titre of 6.52cm3 we musti! ness first work out how many moles of potassium manganate(VII) are used. Moles in a...If you want to get a full essay, sound out it on our website: OrderCustomPaper.com

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